Synthesis of Polyphosphoesters by Esterification or Transesterification Under Microwave Conditions

Author(s): Gheorghe Ilia*, Erika Bálint, György Keglevich

Journal Name: Current Green Chemistry

Volume 5 , Issue 3 , 2018


Become EABM
Become Reviewer
Call for Editor

Graphical Abstract:


Abstract:

Synthesis of polyphosphoesters was accomplished under microwave irradiation by direct esterification or transesterification of phosphonic compounds (acids or esters) in reaction with polyethylene glycol having different molar masses. The polyphosphoesters were characterized by IR and 1H-NMR spectral data. Gel Permeation Chromatography (GPC) with an Evaporative Light Scattering Detector was used to determine the molar weights. The highest molecular weight was ∼8000.

Keywords: Polyphosphoesters, esterification, transesterification, microwave irradiation, phosphonic compound, H-NMR spectral data.

open access plus

Rights & PermissionsPrintExport Cite as

Article Details

VOLUME: 5
ISSUE: 3
Year: 2018
Page: [185 - 190]
Pages: 6
DOI: 10.2174/2213346105666180924121013

Article Metrics

PDF: 38
HTML: 2