Abstract
An efficient procedure of flash heating by microwave irradiation was described for the attachment of 6-O-benzylallosamizoline 8 to chloromethylated Wang resin 7 via its corresponding stannylene intermediate. The reaction rate and loading for compound 8 were significantly enhanced when the microwave irradiation protocol was compared with the conventional heating method.
Keywords: Wang resin-supported 6-O-benzylallosamizoline, synthesis, stannylene method, microwave irradiation, conventional heating method
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