A Convenient and Practical Method for the Synthesis of Aromatic Nthiophosphoryl Imines

Author(s): Xinyuan Xu, Chungui Wang, Zhenghong Zhou, Zebing Zeng, Xinpeng Ma, Guofeng Zhao, Chuchi Tang.

Journal Name: Letters in Organic Chemistry

Volume 3 , Issue 8 , 2006

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Thermal condensation of acetals with different thiophosphoramides at 120-160 °C resulted in the formation of the corresponding N-thiophosphoryl imines in good to excellent yield (80-98%) with high purity ( > 95%, determined by 1H NMR and elemental analyses).

Keywords: N-Thiophosphoryl imine, thermal condensation, thiophosphoramide, acetal

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Article Details

Year: 2006
Page: [640 - 642]
Pages: 3
DOI: 10.2174/157017806778559446
Price: $58

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