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Current Organic Chemistry

Editor-in-Chief

ISSN (Print): 1385-2728
ISSN (Online): 1875-5348

Synthesis, Structural Characterization, Spectroscopic and Electrochemical Studies of N,N-bis[(2,4-dimethoxyphenyl) methylidene]butane-1,4-diamine

Author(s): Mustafa Dolaz, Vickie McKee, Aysegul Golcu and Mehmet Tumer

Volume 14, Issue 3, 2010

Page: [281 - 288] Pages: 8

DOI: 10.2174/138527210790231946

Price: $65

Abstract

In this study, the title compound, N,N-bis[(2,4-dimethoxyphenyl)methylidene]butane-1,4-diamine (L), was prepared and characterized by analytical and spectroscopic methods. The analytical data of the Schiff base ligand (L) confirms the proposed structure. The conductance value indicates that the ligand is non-electrolyte. The electrochemical properties of the ligand (L) are dependent on irreversible and quasi-reversible redox waves in the anodic and cathodic regions, due to oxidation and reduction. The single crystal of the ligand (L) was obtained from MeOH solution. Space group and crystal system of the ligand are P21/C and monoclinic, respectively. Unit cell dimensions of the ligand are a=4.0647(2) Å, b=17.4186 (10) Å, c= 13.8982(8) Å and β= 94.325 (1) .


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