Synthesis, Structural Characterization, Spectroscopic and Electrochemical Studies of N,N-bis[(2,4-dimethoxyphenyl) methylidene]butane-1,4-diamine

Author(s): Mustafa Dolaz , Vickie McKee , Aysegul Golcu , Mehmet Tumer .

Journal Name: Current Organic Chemistry

Volume 14 , Issue 3 , 2010

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In this study, the title compound, N,N-bis[(2,4-dimethoxyphenyl)methylidene]butane-1,4-diamine (L), was prepared and characterized by analytical and spectroscopic methods. The analytical data of the Schiff base ligand (L) confirms the proposed structure. The conductance value indicates that the ligand is non-electrolyte. The electrochemical properties of the ligand (L) are dependent on irreversible and quasi-reversible redox waves in the anodic and cathodic regions, due to oxidation and reduction. The single crystal of the ligand (L) was obtained from MeOH solution. Space group and crystal system of the ligand are P21/C and monoclinic, respectively. Unit cell dimensions of the ligand are a=4.0647(2) Å, b=17.4186 (10) Å, c= 13.8982(8) Å and β= 94.325 (1) .

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Article Details

Year: 2010
Page: [281 - 288]
Pages: 8
DOI: 10.2174/138527210790231946
Price: $58

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