Letters in Organic Chemistry

Miguel Yus  
Universidad de Alicante Apdo
Alicante
Spain

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Mechanically Activated Solid-State Synthesis of Phenylhydrazone Derivatives via High-Speed Ball Milling

Author(s): Xingyi Zhu, Yuanyuan Chen, Yuhe Chen, Jue Wang, Weike Su.

Graphical Abstract:


Abstract:

A series of phenylhydrazone derivatives was synthesized from arenediazonium tetrafluoroborates and active methylene compounds under high-speed ball milling. The reaction occurred in the absence of the solvent and products were obtained in good yield within short reaction times (no more than 30 min).

Keywords: Ball milling, solid-state synthesis, phenylhydrazones, arenediazonium tetrafluoroborates, active methylene compounds.

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Article Details

VOLUME: 11
ISSUE: 8
Year: 2014
Page: [621 - 626]
Pages: 6
DOI: 10.2174/1570178611999140404111411
Price: $58